Cross-coupling reaction between boronic acid & an organohalide
The Suzuki reaction or Suzuki coupling is an organic reaction that uses a palladium complex catalyst to cross-couple a boronic acid to an organohalide .[ 1] [ 2] [ 3] It was first published in 1979 by Akira Suzuki , and he shared the 2010 Nobel Prize in Chemistry with Richard F. Heck and Ei-ichi Negishi for their contribution to the discovery and development of noble metal catalysis in organic synthesis .[ 4] This reaction is sometimes telescoped with the related Miyaura borylation ; the combination is the Suzuki–Miyaura reaction . It is widely used to synthesize polyolefins , styrenes , and substituted biphenyls .
The general scheme for the Suzuki reaction is shown below, where a carbon-carbon single bond is formed by coupling a halide (R1 -X) with an organoboron species (R2 -BY2 ) using a palladium catalyst and a base . The organoboron species is usually synthesized by hydroboration or carboboration , allowing for rapid generation of molecular complexity.
General scheme of Suzuki reaction
Several reviews have been published describing advancements and the development of the Suzuki reaction.[ 5] [ 6] [ 7]
^ Miyaura, Norio; Yamada, Kinji; Suzuki, Akira (1979). "A new stereospecific cross-coupling by the palladium-catalyzed reaction of 1-alkenylboranes with 1-alkenyl or 1-alkynyl halides" . Tetrahedron Letters . 20 (36): 3437–3440. doi :10.1016/S0040-4039(01)95429-2 . hdl :2115/44006 .
^ Miyaura, Norio; Suzuki, Akira (1979). "Stereoselective synthesis of arylated (E)-alkenes by the reaction of alk-1-enylboranes with aryl halides in the presence of palladium catalyst". Chem. Comm. (19): 866–867. doi :10.1039/C39790000866 .
^ Miyaura, Norio ; Suzuki, Akira (1995). "Palladium-Catalyzed Cross-Coupling Reactions of Organoboron Compounds". Chemical Reviews . 95 (7): 2457–2483. CiteSeerX 10.1.1.735.7660 . doi :10.1021/cr00039a007 . S2CID 53050782 .
^ Nobelprize.org. "The Nobel Prize in Chemistry 2010" . Nobel Prize Foundation. Retrieved 2013-10-25 .
^ Suzuki, Akira (1991). "Synthetic Studies via the cross-coupling reaction of organoboron derivatives with organic halides" . Pure Appl. Chem . 63 (3): 419–422. doi :10.1351/pac199163030419 .
^ Miyaura, Norio; Suzuki, Akira (1979). "Palladium-Catalyzed Cross-Coupling Reactions of Organoboron Compounds" . Chemical Reviews . 95 (7): 2457–2483. CiteSeerX 10.1.1.735.7660 . doi :10.1021/cr00039a007 . S2CID 53050782 . (Review)
^ Suzuki, Akira (1999). "Recent advances in the cross-coupling reactions of organoboron derivatives with organic electrophiles, 1995–1998" . Journal of Organometallic Chemistry . 576 (1–2): 147–168. doi :10.1016/S0022-328X(98)01055-9 .